反应 #1178485

反应方程式

Cis-4-tert-butoxycarbonyl-3,5-dimethylmorpholine

hydrochloric acid 1,4-dioxane

→

title compound

Cis-3,5-dimethylmorpholine hydrochloride

反应条件

后处理

1. 1
   浓缩The reaction liquor was concentrated under reduced pressure
2. 2
   其他dried

实验过程

Cis-4-tert-butoxycarbonyl-3,5-dimethylmorpholine g, 8.18 mmol) was dissolved in 4N-hydrochloric acid/1,4-dioxane (50 mL), and the solution was stirred for 3 days at room temperature. The reaction liquor was concentrated under reduced pressure and dried, to obtain the title compound as an oily matter. This compound was used in the subsequent reaction without performing further purification.

来源