反应 #1121771

反应方程式

3-tert-butyldimethylsilyloxybenzoic acid

thionyl chloride

→

3-tert-Butyldimethylsilyloxybenzoyl chloride

反应条件

后处理

1. 1
   温度was heated
2. 2
   温度at reflux for 90 mins
3. 3
   浓缩The reaction mixture was concentrated under reduced pressure
4. 4
   其他to give an oil
5. 5
   其他yield 5.77 parts of the following structure

实验过程

Into a 100 mL round bottom flask a mixture of 5 parts of 3-tert-butyldimethylsilyloxybenzoic acid and 25 mL of thionyl chloride was heated at reflux for 90 mins. The reaction mixture was concentrated under reduced pressure to give an oil, yield 5.77 parts of the following structure.

来源