反应 #1113893

反应方程式

(S)—N-{3-[4-(1-thia-6-aza-spiro[2.5]oct-6-yl)-3-fluorophenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide

sodium periodate

methanol water

→

title compound

收率 57.0%

(S)—N-{3-[4-(1-sulfinyl-6-aza-spiro[2.5]oct-6-yl)-3-fluorophenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide

收率 57.0%

反应条件

后处理

1. 1
   其他at a temperature 25-30° C.
2. 2
   其他for 14 hours

实验过程

The title compound was prepared by reacting (S)—N-{3-[4-(1-thia-6-aza-spiro[2.5]oct-6-yl)-3-fluorophenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide (0.4 mmol) and sodium periodate (mmol) in methanol water mixture (10 ml) at a temperature 25-30° C. for 14 hours in 57% yield.

来源