反应 #1106665

反应方程式

1,8-dichloroanthraquinone

N,N-dimethylethylenediamine

→

Compound 6

1,8-bis(2-(dimethylamino)ethylamino)anthracene-9,10-dione

溶剂

water

反应条件

后处理

1. 1
   温度was refluxed for 18 h
2. 2
   其他to precipitate the title compound which
3. 3
   其他was recrystallised from methanol

实验过程

A mixture of 1,8-dichloroanthraquinone (5.5 g, 20 mmol) and N,N-dimethylethylenediamine (40 mL) was refluxed for 18 h. The mixture was cooled to room temperature and diluted with water to precipitate the title compound which was recrystallised from methanol to afford Compound 6 (4.5 g). The structure of Compound 6 is given below:

来源