反应 #1076776

ord-e33355e07b00435d86bf4f9c7a122aae

反应方程式

[Na+].[OH-]
sodium hydroxide
CCCCCCCCCCCCCCCCCCCCCC(=O)O
behenic acid
CCCCCCCCCCCCCCCCCCCC(=O)O
arachidic acid
CCCCCCCCCCCCCCCCCC(=O)O
stearic acid
O=[N+]([O-])O
nitric acid
→
CCCCCCCCCCCCCCCCCCCCCC(=O)[O-].[Na+]
sodium behenate

反应物

[Na+].[OH-]
sodium hydroxide
CCCCCCCCCCCCCCCCCCCCCC(=O)O
behenic acid
CCCCCCCCCCCCCCCCCCCC(=O)O
arachidic acid
CCCCCCCCCCCCCCCCCC(=O)O
stearic acid
O=[N+]([O-])O
nitric acid

试剂

无

溶剂

O
water

反应条件

温度
55°CELSIUS
详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    workup.STIRRINGstirred for 30 min.

实验过程

In 945 ml water were dissolved 32.4 g of behenic acid, 9.9 g of arachidic acid and 5.6 g of stearic acid at 90° C. Then, after adding 98 ml of 1.5M aqueous sodium hydroxide solution with stirring and further adding 0.93 ml of concentrated nitric acid, the solution was cooled to a temperature of 55° C. and stirred for 30 min. to obtain an aqueous sodium behenate solution.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US06458519B1uspto-grants-2002_10