反应 #1074076

反应方程式

norbornylene

bicyclo[2.2.1]hept-5-ene-2-methanol

maleic anhydride

AIBN

→

title polymer

收率 57.0%

bicyclo[2.2.1]hept-5-ene-2-methanol norbornene maleic anhydride

收率 57.0%

溶剂

tetrahydrofuran

反应条件

后处理

1. 1
   其他The resulting solution was reacted at 67° C. for 8 hours
2. 2
   其他Thereafter, a polymer was precipitated
3. 3
   过滤filtered in petroleum ether/ether (1/1) solution

实验过程

To 70 ml of tetrahydrofuran was added 0.05 M of norbornylene, 0.15 M of bicyclo[2.2.1]hept-5-ene-2-methanol, 0.2 M of maleic anhydride and 0.4 g of AIBN. The resulting solution was reacted at 67° C. for 8 hours. Thereafter, a polymer was precipitated and filtered in petroleum ether/ether (1/1) solution, to obtain the title polymer (yield: 57%).

来源