反应 #1070755

反应方程式

15

2-(N-ethyl-N-phenylamino)ethanol

acetic acid anhydride

→

2-(N-ethyl-N-phenylamino)ethylethanoate

反应条件

后处理

1. 1
   其他equipped with a CaCl2-tube
2. 2
   其他Then, the volatile compounds are evaporated
3. 3
   workup.DISTILLATIONthe crude product is distilled under vacuüm

实验过程

A mixture of 49.6 g (300 mmol) of 15 and 50 ml of acetic acid anhydride in a 250 ml-flask, equipped with a CaCl2-tube is stirred overnight at 60° C. Then, the volatile compounds are evaporated and the crude product is distilled under vacuüm.

来源