反应 #1004999

ord-b13084a291b34f4d927a414582d766a7

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他a softening part of approximately 90°-105°C

实验过程

Para-tert. butyl phenol disulfide is produced by the reaction of para-tert. butyl phenol with sulfur monochloride. When the reaction is carried out using approximately 11:10 moles of phenol to monochloride, the para-tert. butyl phenol disulfide will have about 28% by weight of sulfur and a softening part of approximately 90°-105°C. The para-tert. butyl phenol is produced by the reaction of isobutylene and phenol according to the following scheme: ##SPC2##

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US03968062uspto-grants-1976_07