Реакция #992696
ord-4f35ba68c5da457ab8339458b719f25e
Уравнение реакции
Mucobromic acid
Aminoguanidine bicarbonate
carbon dioxide
→
Aminoguanidinium Mucobromate
Реагенты
Нет
Растворители
Условия реакции
Подробные условия
See reaction.notes.procedure_details.
Обработка
- 1ДругоеThe water was removed in vacuo
- 2Температураwith heating to approximately 90° C
- 3ДругоеThe product was isolated as an off-white solid
Методика
Mucobromic acid (2.0 g, 7.76 mmol) was dissolved in 10 ml of distilled water. Aminoguanidine bicarbonate (1.06 g, 7.76 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 18 hours. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as an off-white solid.