Реакция #992694

Уравнение реакции

Glycolic acid

Guanidine carbonate

carbon dioxide

→

Guanidinium Glycolate

Растворители

water

Условия реакции

Обработка

1. 1
   ДругоеThe water was removed in vacuo
2. 2
   Температураwith heating to approximately 90° C
3. 3
   ДругоеThe product was isolated as a white solid

Методика

Glycolic acid (3.0 g, 39.45 mmol) was dissolved in 15 ml of distilled water. Guanidine carbonate (3.55 g, 19.72 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 4 hours. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as a white solid.

Источник