Реакция #992687

Уравнение реакции

Tetrafluorosuccinic acid

Guanidine carbonate

carbon dioxide

→

Bis(guanidinium) Tetrafluorosuccinate

Растворители

water

Условия реакции

Обработка

1. 1
   ДругоеThe water was removed in vacuo
2. 2
   Температураwith heating to approximately 90° C. for 4 hours
3. 3
   ДругоеThe product was isolated as a white solid

Методика

Tetrafluorosuccinic acid (500 mg, 2.63 mmol) was dissolved in 10 ml of distilled water. Guanidine carbonate (474 mg, 2.63 mmol) was added at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 2 hours. The water was removed in vacuo with heating to approximately 90° C. for 4 hours. The product was isolated as a white solid.

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