Реакция #992679

Уравнение реакции

Hydrazine monohydrate

Trifluoroacetic acid

→

Hydrazinium TFA

Растворители

water

Условия реакции

Обработка

1. 1
   workup.STIRRINGthe reaction was stirred at room temperature overnight
2. 2
   ДругоеThe water was removed in vacuo
3. 3
   Температураwith heating to 80° C.
4. 4
   Другоеyielding product as a colorless liquid

Методика

Hydrazine monohydrate (4.41 ml, 90.9 mmol) was added via syringe to a 250-ml round-bottom flask containing 50 ml of distilled water with stirring at room temperature. Trifluoroacetic acid (7.0 ml, 90.9 mmol) was added via syringe and the reaction was stirred at room temperature overnight. The water was removed in vacuo with heating to 80° C., yielding product as a colorless liquid.

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