Реакция #985245
ord-2770af4c3d4f4844962ba4d053214fb5
Уравнение реакции
Условия реакции
Подробные условия
See reaction.notes.procedure_details.
Обработка
- 1workup.ADDITIONto mixing
- 2ДругоеThe initial solid phase formed immediately
- 3workup.ADDITIONon mixing
- 4Фильтрацияwas filtered
- 5Промывкаwashed (with distilled water+NaOH, pH 10)
- 6Другоеfreeze-dried
Методика
The calcium solution was added rapidly with stirring to the phosphate solution. All solutions were adjusted to pH 10 with concentrated NaOH prior to mixing. The initial solid phase formed immediately on mixing was filtered, washed (with distilled water+NaOH, pH 10), and then freeze-dried.