Реакция #955933

Уравнение реакции

methyl 2,4-dimethylbenzoate

hydrazine

→

2,4-dimethylbenzohydrazide

Растворители

MeOH

Условия реакции

Обработка

1. 1
   Температураthe mixture was heated
2. 2
   Температураunder reflux for 40 hours
3. 3
   ДругоеThen the mixture was evaporated
4. 4
   Другоеdried under vacuum

Методика

To a solution of methyl 2,4-dimethylbenzoate (2 g, 12.2 mmol) in MeOH (10 mL) was added anhydrous hydrazine (1.95 mL, 61 mmol) and the mixture was heated under reflux for 40 hours. Then the mixture was evaporated and dried under vacuum to give 2,4-dimethylbenzohydrazide as a white solid (2 g, 100%; MS (M+H, 165).

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