Реакция #955906

Уравнение реакции

hydrazine monohydrate

3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy nitrobenzene

→

3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy aniline

Выход 71.4%

Растворители

ethanol

Условия реакции

Обработка

1. 1
   Температураvia heat-refluxing for 24 hours
2. 2
   ДругоеVia recrystallized
3. 3
   workup.ADDITIONfrom mix solution of chloroform-methanol

Методика

Thereafter, loaded were 3 ml of hydrazine monohydrate and 10 ml of ethanol in the presence of graphite, 3.9 g of 3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy nitrobenzene was reduced via heat-refluxing for 24 hours. Via recrystallized from mix solution of chloroform-methanol to obtain 2.7 g of 3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy aniline (yield: 71%).

Источник