Реакция #94102

Уравнение реакции

dimethyl adipate

sodium hydroxide

→

disodium adipate

Растворители

acetonitrile

Условия реакции

Обработка

1. 1
   Температураat reflux temperature for 18 hours
2. 2
   ФильтрацияThe resulting solution was filtered hot
3. 3
   Другоеdried

Методика

17.4 g. (0.1 mole) of dimethyl adipate were dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 g. (0.2 mole) of 97% pure sodium hydroxide were added to the reaction mixture as a fine powder (50 mesh). The reaction mixture was stirred at reflux temperature for 18 hours. The resulting solution was filtered hot and the solids were air dried to yield disodium adipate as the reaction product.

Источник