Реакция #9346

Уравнение реакции

Sodium propanoate

2,6-dipropylphenol

→

phenol

2,6-dipropyl-4-propionylphenol

Растворители

Triflic Acid

Условия реакции

Обработка

1. 1
   ДругоеThe resulting waxy solid was purified by chromatography on silica gel

Методика

Sodium propanoate (0.88 g, 1.5 eq) and 2,6-dipropylphenol (1.09 g, 1.0 eq) were combined in Triflic Acid (5.0 g) as in Example 13, step 1. The resulting waxy solid was purified by chromatography on silica gel using ethyl acetate:hexanes:acetic acid (10:90:1) to give the titled phenol.

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