Реакция #91963

Уравнение реакции

3-methyl-4-[(2-methylpropan-2-yl)oxycarbonyl]morpholine-3-carboxylic acid

trifluoroacetic acid

→

3-methylmorpholine-3-carboxylic acid

Растворители

DCM

Условия реакции

Обработка

1. 1
   Концентрированиеconcentrated under the vacuum
2. 2
   ДругоеThe residue was used directly in next step without further purification

Методика

To a solution of 3-methyl-4-[(2-methylpropan-2-yl)oxycarbonyl]morpholine-3-carboxylic acid (Accela ChemBio Co., Ltd., CAS: 1052680-53-1, 50 mg, 0.2.0 mmol) in DCM (1 ml) was added trifluoroacetic acid (1 mL) dropwise at room temperature. The resulting mixture was stirred at room temperature for one hour and then concentrated under the vacuum. The residue was used directly in next step without further purification,

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