Реакция #89798

ord-1afbf282da9749e4968987763070ad89

Уравнение реакции

CCCCC(CC)CNCC(CC)CCCC
2,2′-diethylhexylamine
CC(Br)C(=O)Cl
2-bromopropionyl chloride
CCCCC(CC)CN(CC(CC)CCCC)C(=O)C(C)Br
2-bromo-N,N-bis(2-ethylhexyl)propanamide
Выход 98.0%

Реагенты

Нет

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Методика

Step A is conducted starting with 2,2′-diethylhexylamine and 2-bromopropionyl chloride and leads to 2-bromo-N,N-bis(2-ethylhexyl)propanamide (Yield: 98%) for which the 1H and 13C NMR characterisations are the following:

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US09441285B2uspto-grants-2016_09