Реакция #82144
ord-165c21acb8a34d9c9681683a969f54e5
Уравнение реакции
Реактанты
Реагенты
Нет
Растворители
Условия реакции
Подробные условия
See reaction.notes.procedure_details.
Обработка
- 1ФильтрацияThe polymer was filtered
- 2ЭкстракцияThe ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor
- 3Другоеdried
- 4Другоеto afford a pale brown solid which
Методика
The resulting heterogeneous reaction mixture, which was lumpy and hardened, was neutralized by addition of 15% aqueous tartaric acid solution. The polymer was filtered and a small portion was ground thoroughly. The ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor and dried to afford a pale brown solid which was not soluble to any extent in distilled water.