Реакция #81041

ord-fc07395c622945258f6551f71b391f76

Уравнение реакции

CCCCCCCCCCCCCCCCCCCCCCCCCCOC(=O)CS(=O)(=O)O.[Na]
sodium lauryl-myristyl sulfoacetate
O=C(O)CCl
monochloroacetic acid
→
CCCCCCCCCCCCCCCCCCCCCCCCCCOC(=O)CCl
Lauryl-myristyl Chloroacetate

Реактанты

CCCCCCCCCCCCCCCCCCCCCCCCCCOC(=O)CS(=O)(=O)O.[Na]
sodium lauryl-myristyl sulfoacetate
O=C(O)CCl
monochloroacetic acid

Реагенты

Нет

Условия реакции

Температура
93°CELSIUS
Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    Температураmaintained at a temperature of between 90° C. and 97° C. for about 11 hours

Методика

The reactor is then heated to a temperature of 93° C. and maintained at a temperature of between 90° C. and 97° C. for about 11 hours. HPLC analysis of the resulting slurry indicates that the sodium lauryl-myristyl sulfoacetate is substantially free of monochloroacetic acid and its salts.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US05616782uspto-grants-1997_04