Реакция #75693

ord-eb3b5948b8064207bc191357b8dc9e1b

Уравнение реакции

Nc1cc(Cl)c(Cl)cc1Cl
2,4,5-trichloroaniline
O=CC(=O)O
glyoxylic acid
C1=COCC1
2,3-dihydrofuran
→
O=C(O)C1Nc2c(Cl)cc(Cl)c(Cl)c2C2OCCC12
Compound 67
O=C(O)C1Nc2c(Cl)cc(Cl)c(Cl)c2C2OCCC12
6,8,9-trichloro-2,3,3a,4,5,9b-hexahydro-furo[3,2-c]quinoline-4-carboxylic Acid

Реактанты

Nc1cc(Cl)c(Cl)cc1Cl
2,4,5-trichloroaniline
O=CC(=O)O
glyoxylic acid
C1=COCC1
2,3-dihydrofuran

Реагенты

Нет

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Методика

Compound 67 was prepared from 2,4,5-trichloroaniline, glyoxylic acid and 2,3-dihydrofuran by the automated process.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US06699877B2uspto-grants-2004_03