Реакция #75255

Уравнение реакции

product

Ethyl 4-(4-Acetyl-8-acetoxy-9-propoxynonyl)benzoate

ethyl 4-(4-acetyl-8-acetoxytridecyl)benzoate

→

4-(4-Acetyl-8-hydroxy-9-propoxynonyl)benzoic Acid

Условия реакции

Обработка

1. 1
   ДругоеThis compound is prepared by the method
2. 2
   ДругоеThe title compound is purified by column chromatography on silica gel with 4% methanol in chloroform as the eluant

Методика

This compound is prepared by the method described in Example 1, Step F, except that the product of Step C of the present example replaces ethyl 4-(4-acetyl-8-acetoxytridecyl)benzoate. The title compound is purified by column chromatography on silica gel with 4% methanol in chloroform as the eluant. The title compound is a light yellow, viscous oil.

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