Реакция #74686

Уравнение реакции

triphenylphosphine

chloromethyl ethyl ether

→

(Ethoxymethyl)triphenylphosphonium chloride

Растворители

benzene

Условия реакции

Обработка

1. 1
   ТемператураThe mixture then was chilled
2. 2
   Фильтрацияfiltered
3. 3
   Другоеto give 7

Методика

A solution of 99.66 g of triphenylphosphine and 37.82 g of chloromethyl ethyl ether in 240 ml of dry benzene was stirred and refluxed (84° C.) for 6 hours. The mixture then was chilled and filtered to give 7, as a white solid, mp 205°-206° C.

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