Реакция #733744

ord-8115ca2de6e944ad8ff0d4db6fcb7e03

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    ДругоеThis compound was prepared
  2. 2
    Другоеreacted

Методика

This compound was prepared using the general Sonagashira procedure as described in the General Procedures Example C. The starting material was N-(4-fluoro-2-iodo-5-trifluoromethyl-phenyl)-methanesulfonamide (0.77 g, 2.0 mmol) and 1-ethylsulfanyl-2-methyl-but-3-yn-2-ol (0.29 g, 2.0 mmol), reacted to yield the title compound as a golden oil.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US07705147B2uspto-grants-2010_04