Реакция #722725

ord-d546c0be93c5496da77831fb43df7de5

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    Другоеthe precipitated product is recrystallized from benzene

Методика

The 3-chloro-4-fluoroacetophenone is then reacted with an aqueous solution of sodium hypobromite, the aqeuous phase is treated with sodium hydrogensulfite and acidified with hydrochloric acid, and the precipitated product is recrystallized from benzene. 3-Chloro-4-fluorobenzoic acid obtained in a yield of 74%.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US06187952B1uspto-grants-2001_02