Реакция #70906

ord-0d0bda2a4ecf4b5fa1825fca2cb4ad7b

Реагенты

Нет

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    Температураto reflux for 2 h
  2. 2
    Концентрированиеconcentrated
  3. 3
    ДругоеThe product obtained

Методика

A solution of isonicotinic acid (0.10 g, 0.8 mmol) and thionyl chloride (1 mL) were heated to reflux for 2 h and concentrated. The product obtained was used immediately in the following step.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US08536194B2uspto-grants-2013_09