Реакция #70520

Уравнение реакции

Phenylmethyl 4-acetyl-2-morpholinecarboxylate

→

title compound

Выход 24.3%

4-Acetyl-2-morpholinecarboxylic acid

Выход 24.3%

Растворители

ethanol

ethanol

Условия реакции

Обработка

1. 1
   Другоеto give the starting material

Методика

Phenylmethyl 4-acetyl-2-morpholinecarboxylate (313 mg, 1.189 mmol) was dissolved in ethanol (5 ml) and hydrogenated at 30 bar on H-Cube using 10% palladium on carbon. The mixture was blown to dryness under a stream of nitrogen to give the starting material. The starting material was dissolved in ethanol (5 ml) and hydrogenated at 50 bar on H-Cube using10% palladium on carbon. The mixture was blown to dryness under a stream of nitrogen to give the title compound (50 mg) as a colourless oil.

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