Реакция #69035

Уравнение реакции

2-Phthalimidoethanesulfonyl chloride

ammonia

→

title compound

2-phthalimidoethanesulfonamide

Растворители

water

dioxane

Условия реакции

Обработка

1. 1
   Другоеthe solution obtained this way

Методика

2-Phthalimidoethanesulfonyl chloride (2.0 g) was added portion wise to a solution of 0.5 M of ammonia in dioxane (15 ml) and the solution obtained this way was stirred at room temperature. After 48 hours the reaction mixture was poured in water (50 ml) causing the title compound to precipitate. The product was collected by filtration. Yield: 1.52 g (83%) of a solid. 1H-NMR (DMSO-δ6) δ (ppm) 7.92-713 (m, 4H), 7.06 (s, 2H), 6.88-3.93 (m, 2H), 3.37-3.30 (m, 2H).

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