Реакция #684948

Уравнение реакции

Thionyl chloride

4-n-butylbenzyl alcohol

→

title compound

Выход 104.9%

1-(Chloromethyl)-4-n-butylbenzene

Выход 104.9%

Растворители

ether

Условия реакции

Обработка

1. 1
   ДругоеAfter concentration of the mixture, excess thionyl chloride was removed by azeotropic distillation with benzene

Методика

Thionyl chloride (2.5 ml, 34 mmol) was added to a solution of 4-n-butylbenzyl alcohol (2.0 g, 12 mmol) in ether (25 ml), and this mixture was stirred at room temperature for 3 hours. After concentration of the mixture, excess thionyl chloride was removed by azeotropic distillation with benzene to give the title compound (2.3 g). This compound was used in the following reaction without purification.

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