Реакция #6683

Уравнение реакции

[R]-1-trifluoromethylheptyl 4-benzyloxybenzoate

→

[R]-1-Trifluoromethylheptyl 4-hydroxybenzoate

Выход 99.0%

Растворители

ethyl acetate

Условия реакции

Обработка

1. 1
   ФильтрацияThen the catalyst was filtered out
2. 2
   Другоеfiltrate was evaporated to dryness
3. 3
   Другоеto give the pure compound in yield of 99%

Методика

2.2 g of [R]-1-trifluoromethylheptyl 4-benzyloxybenzoate, (13) 100 mg of PdOH/C in 50 ml of ethyl acetate was stirred at RT over night under H2 atmosphere. Then the catalyst was filtered out and filtrate was evaporated to dryness to give the pure compound in yield of 99%.

Источник