Реакция #65034

ord-947c77284e834395add5a41dba46ce12

Уравнение реакции

Fc1c(F)c(F)c(B(c2c(F)c(F)c(F)c(F)c2F)c2c(F)c(F)c(F)c(F)c2F)c(F)c1F.O.O.O

→

Реактанты

(C6F5)3B.3H2O

(C6F5)3B

Реагенты

Нет

Растворители

dichloromethane

Условия реакции

Подробные условия

See reaction.notes.procedure_details.

Обработка

1
Другоеevaporated to dryness under vacuum

Методика

A mixture of 0.566 gram (1 mmol) (C6F5)3B.3H2O as prepared in Example 1 and 1.024 grams (2 mmol) (C6F5)3B in 10 mL dichloromethane was stirred for 15 minutes and then evaporated to dryness under vacuum. A quantitative yield of the product remained and was stored under dry nitrogen.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US05416177uspto-grants-1995_05