Реакция #649

Уравнение реакции

Cn1nc(Br)nc1Br

CN1CCNCC1

→

CN1CCN(c2nc(Br)nn2C)

Растворители

Cc1ccccc1

Условия реакции

Методика

A mixture of 3,5-dibromo-1-methyl-1H-1,2,4-triazole (142 mg, 0.59 mmol), 1-methylpiperazine (62.0 mg, 0.62 mmol), tris(dibenzylideneacetone)dipalladium(0) (81 mg, 0.09 mmol), BINAP (110 mg, 0.18 mmol) and sodium tert-butoxide (113 mg, 1.18 mmol) in toluene (8 ml) was stirred at 100 °C for 1.5hrs. LCMS indicated no desired product formation. Discarded.

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