Реакция #64731

Уравнение реакции

ethyl 1,1-diethoxyethylphosphinate

methylmagnesium chloride

potassium carbonate

→

methyl (1,1-diethoxyethyl)phosphine oxide

Растворители

water

Условия реакции

Обработка

1. 1
   Другоеto precipitate inorganic salts

Методика

By a procedure analogous to that of Example 1, but using ethyl 1,1-diethoxyethylphosphinate (10.5 g) and 33.5 ml of the methylmagnesium chloride solution and adding 14.1 g of potassium carbonate in 30 ml of water to precipitate inorganic salts, methyl (1,1-diethoxyethyl)phosphine oxide is obtained as a colourless oil.

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