Реакция #640569

Уравнение реакции

diethyl ether

thioanisole

dimethyl sulfate

→

dimethylphenylsulfonium sulfate

Растворители

water

water

Условия реакции

Методика

At room temperature, 6.2 g (0.05 mole) of thioanisole and 6.9 g (0.055 mole) of dimethyl sulfate were stirred for 12 hours. To the reaction solution were added 100 g of water and 50 ml of diethyl ether. The water layer was taken out, obtaining an aqueous solution of the desired dimethylphenylsulfonium sulfate.

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