Реакция #640563

Уравнение реакции

2-aminophenylboronic acid

acryloyl chloride

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2-Acrylamido-phenylboronic acid

Условия реакции

Обработка

1. 1
   ЭкстракцияThe product was extracted in acetone
2. 2
   Другоеdried
3. 3
   Другоеa rotary evaporator

Методика

2-Acrylamido-phenylboronic acid (“2-APB”) was synthesized by reacting 2-aminophenylboronic acid with an excess of acryloyl chloride in an aqueous alkaline solution. The product was extracted in acetone and dried using a rotary evaporator. The structure of 2-APB was confirmed using NMR. The purity was shown to be greater than 90%.

Источник