Реакция #640562

Уравнение реакции

3-amino phenylboronic acid

acryloyl chloride

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3-Acrylamido-phenylboronic acid

Условия реакции

Обработка

1. 1
   ЭкстракцияThe product was extracted in acetone
2. 2
   Другоеdried
3. 3
   Другоеa rotary evaporator

Методика

3-Acrylamido-phenylboronic acid (“3-APB”) was synthesized by reacting 3-amino phenylboronic acid with an excess of acryloyl chloride in an aqueous alkaline solution. The product was extracted in acetone and dried using a rotary evaporator. The structure of 3-APB was confirmed using NMR. The purity was about 90%, TLC showing very little contamination.

Источник