Реакция #640553

Уравнение реакции

Hexyltrimethylammonium hydroxide

tetraethylorthosilicate

→

Hexyltrimethylammonium Silicate

Растворители

water

Условия реакции

Обработка

1. 1
   ДругоеAfter hydrolysis
2. 2
   Другоеthe solution was placed on a rotary evaporator
3. 3
   Другоеto remove the alcohol
4. 4
   ДругоеA total of 518.6 g of liquid was removed
5. 5
   workup.ADDITIONafter which 150 g of deionized water was added

Методика

Hexyltrimethylammonium hydroxide, (30.03%), 492.96 g, was diluted with 1073.86 g deionized water and to it there were added 650.0 g of tetraethylorthosilicate, (98%) with stirring. After hydrolysis was complete, the solution was placed on a rotary evaporator to remove the alcohol. A total of 518.6 g of liquid was removed, after which 150 g of deionized water was added. Elemental analysis showed the solution to contain 5.10 wt % Si.

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