Реакция #631971

Уравнение реакции

2-Carboxyethyl acrylate

Thionyl chloride

→

desired product

3-chloro-3-oxopropyl acrylate

Растворители

CH2Cl2

Условия реакции

Обработка

1. 1
   Температураthe solution is cooled in an ice bath
2. 2
   ДругоеThe solvent is removed under reduced pressure

Методика

2-Carboxyethyl acrylate (1 eq.) is dissolved in CH2Cl2 and the solution is cooled in an ice bath. Thionyl chloride (1 eq.) is added dropwise and the mixture is allowed to warm to room temperature and stir for 4 hours. The solvent is removed under reduced pressure and the desired product is isolated by vacuum distillation.

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