Реакция #630170

Уравнение реакции

N-phosphonomethylglycine

hydrochloric acid

→

N-phosphonomethylglycine hemihydrochloride hemihydrate

Условия реакции

Обработка

1. 1
   ДругоеAfter the exothermic reaction
2. 2
   ПромывкаThe crystalled solid was washed with tetrahydrofuran
3. 3
   Другоеair-dried

Методика

N-phosphonomethylglycine (10 g.) was placed in a small beaker and covered with concentrated hydrochloric acid (approximately 5 ml.). After the exothermic reaction had subsided, the mixture was allowed to stand about 10 to 15 minutes. The crystalled solid was washed with tetrahydrofuran and then air-dried to yield an essentially quantitative yield of N-phosphonomethylglycine hemihydrochloride hemihydrate (m.p. greater than 300° C.).

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