Реакция #62841

ord-72725f58058848e5b39d0da2169d49e7

Уравнение реакции

CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)O
3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid
CN(C)CCN
N,N-dimethylethylene diamine
→
CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)NCCN(C)C
title compound
Выход 88.0%
CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)NCCN(C)C
N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-N',N'-dimethylethylenediamine
Выход 88.0%

Реактанты

CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)O
3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid
CN(C)CCN
N,N-dimethylethylene diamine

Реагенты

Нет

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Методика

The procedure of Example 9 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid and 3.3 ml of N,N-dimethylethylene diamine were used as starting materials. 6.5 g (yield 88%) of the title compound was obtained as a pale yellow oil.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US04762829uspto-grants-1988_08