Реакция #61209

ord-d38bdd28172f4dbcb04b810c551498b3

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    ДругоеThis compound was prepared
  2. 2
    Другоеreacted

Методика

This compound was prepared using the standard Sonagashira procedure as described in General Procedures Example C. The starting material was N-(2-iodo-4-nitro-5-trifluoromethyl-phenyl)-methanesulfonamide (0.34 g, 0.82 mmol) and 4-ethylsulfanyl-3-methoxy-3-methyl-but-1-yne (0.13 g, 0.82 mmol), reacted to yield the title compound as a yellow film.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US07427682B2uspto-grants-2008_09