Реакция #595369

Уравнение реакции

methyl 4-(benzyloxy)-2-(prop-1-en-2-yl)benzoate

→

title compound

methyl 4-hydroxy-2-isopropylbenzoate

Растворители

methanol

Условия реакции

Обработка

1. 1
   ФильтрацияThen the mixture was filtered
2. 2
   Концентрированиеthe filtrate was concentrated

Методика

To a solution of methyl 4-(benzyloxy)-2-(prop-1-en-2-yl)benzoate (i-1d) (4.6 g, 16.3 mmol) in methanol (100 ml) was added Pd/C (0.46 g). The mixture was stirred at rt under H2 atmosphere for 24 h. Then the mixture was filtered, and the filtrate was concentrated to afford the title compound. LCMS (ESI) calc'd for C11H14O3 [M+H]+: 195.1. found: 195.1.

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