Реакция #590865

ord-77e39507b01e4e5c972bac83a24bbb9b

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    Другоеreacted for 2 hours at 80° C
  2. 2
    Другоеreacted for 3 hours at 80° C.

Методика

1000 g of polyethylene glycol having a molecular weight of about 2,000 and 168 g (1 mole) of hexamethylene diisocyanate were placed in a reaction vessel and reacted for 2 hours at 80° C. Moreover, 116 g (1 mole) of 2-hydroxyethyl acrylate and 4.7 g of hydroquinone were added thereto and reacted for 3 hours at 80° C. while blowing in air to obtain a urethane acrylate (A-1) having acryloyl groups on both ends of a molecule thereof. The weight average molecular weight of the urethane acrylate (A-1) was 3,800.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US07776937B2uspto-grants-2010_08