Реакция #54949

ord-21f595ce2255497e8b72055a7472fa8b

Реагенты

Нет

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    Другоеa temperature of 100° C.
  2. 2
    Другоеyield on the theoretical value=50%)
  3. 3
    Другоеat 185°-186° C.
  4. 4
    Другоеwere obtained

Методика

By operating according to Example 13, but using anisole as the solvent and a temperature of 100° C., and starting from 15.1 g of 3-acetylaminophenol, 9.0 g of a product (yield on the theoretical value=50%) having a melting point at 185°-186° C. were obtained.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US04151201uspto-grants-1979_04