Реакция #53679

Уравнение реакции

3,5-diamino-1H-indazole

pyridine

2,6-dichlorobenzenesulfonyl chloride

→

N-(3-amino-1H-indazol-5-yl)-2,6-dichlorobenzenesulfonamide

Выход 18.6%

Растворители

tetrahydrofuran

Условия реакции

Методика

N-(3-Amino-1H-indazol-5-yl)-2,6-dichlorobenzenesulfonamide can be obtained as described in Example 39 from 0.8 g of 3,5-diamino-1H-indazole, 8 ml of pyridine, 8 ml of tetrahydrofuran and 1.29 g of 2,6-dichlorobenzenesulfonyl chloride. 350 mg of N-(3-amino-1H-indazol-5-yl)-2,6-dichlorobenzenesulfonamide are thus obtained in the form of a pale yellow solid melting at 250° C. (analysis C13H10Cl2N4O2S % calculated C, 43.71; H, 2.82; Cl, 19.85; N, 15.68; O, 8.96; S, 8.98. % found C, 43.39; H, 2.92; Cl, 19.45; N, 15.31; S, 8.73).

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