Реакция #531791

Уравнение реакции

Mercaptopropionic acid

Triphenylmethylchloride

→

3-(tritylthio)propionic acid

Выход 95.7%

Растворители

methylene chloride

Условия реакции

Обработка

1. 1
   Другоеwere carried out at room temperature
2. 2
   Фильтрацияwas gathered by filtration
3. 3
   Другоеthe solid components obtained here
4. 4
   Другоеwere dried under reduced pressure

Методика

Mercaptopropionic acid 12 (3.14 g) was dissolved in 50 ml of methylene chloride. Triphenylmethylchloride 13 (8.36 g) was added to that, and 19-hour reactions were carried out at room temperature. The precipitate generated through the reactions was gathered by filtration, and the solid components obtained here were dried under reduced pressure, to form 9.86 g of 3-(tritylthio)propionic acid 14, which is a white solid.

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