Реакция #52601

Уравнение реакции

dimethyl-3-nitrobiphenyl-4-malonate

→

3-nitrobiphenyl-4-acetic acid

Растворители

hydrochloric acid

Условия реакции

Обработка

1. 1
   ФильтрацияThe precipitate was collected by filtration
2. 2
   Промывкаwashed with water
3. 3
   Другоеdried

Методика

Crude dimethyl-3-nitrobiphenyl-4-malonate was refluxed in 30 mL of 6 N hydrochloric acid for 24 hours. The precipitate was collected by filtration, washed with water and dried to give 4.5 g of 3-nitrobiphenyl-4-acetic acid as a cream colored solid.

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