Реакция #5223

ord-dcadfe0e1eca4e47a8b88dad58fe8309

Реагенты

Нет

Растворители

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    workup.STIRRINGThereafter, the mixture was stirred at room temperature for 19 hours

Методика

2-Aminoethanol (13.76 g, 225.3 mmol) was dissolved in CHCl3 (750 ml). To the solution was added dropwise palmitoyl chloride (15.48 g, 56.3 mmol) with stirring under ice cooling. Thereafter, the mixture was stirred at room temperature for 19 hours.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US05243035uspto-grants-1993_09