Реакция #518022

Уравнение реакции

N-butylidenebutylamine

ethyl diazoacetate

ethanol

→

1-butyl-2-ethoxycarbonyl-3-propylaziridine

Выход 30.0%

Условия реакции

Методика

A mixture of 0.5 mmol of N-butylidenebutylamine, 0.5 mmol of ethyl diazoacetate, 0.015 mmol of di-μ-chlorotetrakis(cyclooctene)diiridium(I) [Ir2Cl2(cyclooctene)4] , and 0.5 ml of ethanol was stirred at room temperature (250° C.) in an argon atmosphere for 3 hours to yield 1-butyl-2-ethoxycarbonyl-3-propylaziridine in a yield of 30%.

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